This book takes the experimental teaching of pharmaceutical chemistry as the starting point, analyzes the safety knowledge of the experimental operation of pharmaceutical chemistry, experimental operation criteria and some methods required by the experimental experiment of pharmaceutical analysis (separation and purification of drugs, ingredient identification, reagent preparation), etc., and provides some ideas for the reform of the experimental teaching of pharmaceutical chemistry. The course of pharmaceutical chemistry experiment has been carried out for many years, and some teaching experience has been accumulated through years of practice. In the teaching process, we should pay attention to step by step, teach students according to their aptitude, pay attention to the initiative and enthusiasm of students, and pay attention to the interaction between teachers and students, which can stimulate the creativity of teachers and the improvement of their own scientific research quality, and also improve the initiative of students. 

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